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M. , 7989, 30, 7095. ; Yamamoto. H . , 7989, 30, 3967. Me, Me I n-C8H17CHO:TiC14 OH -5OoC, 2h - 61% 48% ee S I Chan. Y; Wang, D. , 7989, 30, 3041. MeCH=CHCHC12 p h w C H o CCl2, THF , DMF 25'C, 2h P- h - OH Me EZ = 9614 anti:syn = 9 3 7 CI Takai. K; Kataoka, Y . ;Ytimoto. K. , 7989, 30, 4389. ; Srebn ik. C. , 1989, 30, 5581. ; Suzuki, H. J. Chern. , Chern. , 1989, 1700. 25OC \" CI p 3. PhCH2CHO 4. 5 1) 8x0 Collins. ; Hong, Y. J. Org. , 1989, 54, 4154. ; Sibille, S . ; Perichon, J. J. Org. , 7989, 54, 2198.

Angew. Chem. Int. , 7989,28, 320. 5 H20 R~C12(PPh3)3, RT Ph 24h Khai. FLT,; Arcelli, A. J. Org. , 7989, 54, 949. BnEt3NCl, NaBH4 aq. THF, 1% Montmorillonite clay aq. NaHCq &&ar. M. Synth. , 7989,79, 2313. 9 6 Oo/ 44 COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 7 Ph ph ZnCl2, Zno , EtOH , 1h * ref lux 4 f0 Toda. ; Tange, H. J. Chem. ,Perkin Trans. I, 1989, 1555. ; Bakthavatchalam, R . ; m . R ~ BOrg. Prep. Proceed. , 1989, 21, 373. ; Perichon, J. , 1987, 28, 5 5 . phmph 1 . ; Chikamatsu, H. J. Chem.

10% aq. ; Virard, C. , 7988,29, 1021. ; Matsuda, H. J. Chem. , Chem. , 7988, 882. ; Graziani, M. , 7989, 30, 2705. NaBH4 (solid state) PhJ Ph PhJ 3d Ph 63% Toda. ; Yagi, M. Angew. Chem. Int. , 7989,28, 320. 5 H20 R~C12(PPh3)3, RT Ph 24h Khai. FLT,; Arcelli, A. J. Org. , 7989, 54, 949. BnEt3NCl, NaBH4 aq. THF, 1% Montmorillonite clay aq. NaHCq &&ar. M. Synth. , 7989,79, 2313. 9 6 Oo/ 44 COMPENDIUM OF ORGANIC SYNTHETIC METHODS VOL 7 Ph ph ZnCl2, Zno , EtOH , 1h * ref lux 4 f0 Toda. ; Tange, H. J.

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